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Title:ONE POT SYNTHESIS AND SUBSEQUENT CHARACTERISATION OF THE LEAD CHALCOGENIDES
DOI No:10.1142/9789812701947_0073
Source:PHYSICS, CHEMISTRY AND APPLICATION OF NANOSTRUCTURES (pp 333-336)
Author(s):S. G. HICKEY
Institut für Physikalische Chemie, Universität Hamburg, Grindelallee 117, D-20146 Hamburg, Germany

M. NAGEL
Institut für Physikalische Chemie, Universität Hamburg, Grindelallee 117, D-20146 Hamburg, Germany

J. NIEHAUS
Institut für Physikalische Chemie, Universität Hamburg, Grindelallee 117, D-20146 Hamburg, Germany

H. WELLER
Institut für Physikalische Chemie, Universität Hamburg, Grindelallee 117, D-20146 Hamburg, Germany

Abstract:A general synthetic strategy for the synthesis of PbX (X = S, Se, Te) is introduced. The resulting material qualities of size and monodispersity are discussed with respect to the injection temperature, growth temperature, growth time and solvent mixture. Some material characterisation data gathered with the aid of transmission electron microscopy (TEM), X-ray diffraction (XRD) and optically using absorbance and emission spectroscopy are presented and discussed.
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